A 'full' spectrum is one that covers chemical shifts from -0.5 to about +10 ppm. Nearly all protons produce signals in this range, so the presence (and absence) of signals in this range is very meaningful.
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Chemistry computer lab printing tips: I have printed from SpinWorks using my office computer and my office printer, but I have not had the same luck in the Chemistry computer lab. At this point in time (Oct 2005), it is necessary for computer lab users to print their SpinWorks spectrum indirectly. This can be done in multiple ways: by 'printing' a PDF file and then making a hard copy of the PDF file, or by transferring the data to MS Word and making a hard copy of the Word document. All three printing options, direct printing (not possible in the computer lab), printing via PDF, and printing via Word, are described below. Use whatever works at your location.
Option #1: direct printing from SpinWorks (from sites outside the Chemistry computer lab):
- Adjust the horizontal scale so that a full spectrum is visible
- Adjust the vertical scale so that the top of the tallest important peak is visible
- If you want to enter a caption or title,
- click Edit: Plot Title
- type your text in the box
- click OK
- Click File: Print Preview
- Troubleshooting: Does the horizontal scale cover the full spectrum? Is the top of the tallest peak visible? Is your spectrum overloaded with peak pick and/or integral data? If any problems are seen, click Close and make necessary corrections.
- Click Print
- click OK
Tutorial note: This ends the step-by-step guide through the tutorial. At this point, you can choose between the following: save your data and quit SpinWorks, or add more data to your spectrum (peak picks, integrals, inset boxes) and print expanded spectra. To get instructions for the latter, select a section from the Table of Contents.
Option #2: printing via CutePDF Writer + Foxit Reader (in the Chemistry computer lab):
To print on the lab printer, you must first create a PDF file by 'printing' your spectrum with CutePDF Writer. Then you need to log in to the lab printer (Clab), open the PDF file in Foxit Reader, and print the PDF file from Foxit Reader. You are billed for your printing on Clab, so make sure you log out of the computer after you are done using SpinWorks (otherwise the next user will be able to charge their printing to you).
- Adjust the horizontal scale so that a full spectrum is visible
- Adjust the vertical scale so that the top of the tallest important peak is visible
- If you want to enter a caption or title,
- click Edit: Plot Title
- type your text in the box
- click OK
- Click File: Print Preview
- Troubleshooting: Does the horizontal scale cover the full spectrum? Is the top of the tallest peak visible? Is your spectrum overloaded with peak pick and/or integral data? If any problems are seen, click Close and make necessary corrections.
- Click Print
- change the printer in the Name: box to CutePDF Writer
- click OK
- select the My Documents folder, give your PDF file a meaningful name, and click Save
- To print this file in the Chemistry computer lab, log in to the Clab printer:
- Double-click on the desktop icon Print Server
- Enter your login and password
- Find your PDF file in the My Documents folder
- double-click on your file (this opens the file in Foxit Reader)
- click File: Print
- select class_lab_printClab from the Printer Name menu
- click OK
- Close Foxit Readerand return to SpinWorks for more processing
It might be a good idea to save your PDF file (you can email it to yourself) so that you can print and/or adjust it later as needed.
Tutorial note: This ends the step-by-step guide through the tutorial. At this point, you can choose between the following: save your data and quit SpinWorks, or add more data to your spectrum (peak picks, integrals, inset boxes) and print expanded spectra. To get instructions for the latter, select a section from the Table of Contents.
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Option #3:printing via MS Word (in the Chemistry computer lab)
To print on the lab computer, you must log in to the printer (Clab), start MS Word and setup the page, copy data from SpinWorks to MS Word, and then print the MS Word document. You are billed for your printing on Clab, so make sure you log out of the computer after you are done using SpinWorks (otherwise the next user will be able to charge their printing to you).
- Make the desktop visible
- Double-click on the desktop icon Print Server
- Enter your login and password
- Start MS Word
- Click File: Page Setup
- Set for landscape mode
- Set all margins to 0.1 inches.
- MS Word will tell you that these margins are too small and will offer to 'fix' them for you. Click on Fix
- Return to SpinWorks
- Adjust the horizontal scale so that a full spectrum is visible
- Adjust the vertical scale so that the top of the tallest important peak is visible
- If you want to enter a caption or title,
- click Edit: Plot Title
- type your text in the box
- click OK
- Click Edit: Copy Metafile to Clipboard
- Return to MS Word
- Click Edit: Paste
- Troubleshooting #1: Does the horizontal scale cover the full spectrum? Is the top of the tallest peak visible? Is your spectrum overloaded with peak pick and/or integral data? To fix these problems, delete the image in MS Word, return to SpinWorks and make necessary corrections, then repeat the Copy-and-Paste steps.
- Troubleshooting #2: Does the spectrum use the entire page in MS Word or is it too small/large? If necessary, adjust the physical size of the picture in MS Word by doing the following:
- Click on image in MS Word
- Click Format: Picture
- Select Size tab
- If necessary, click Lock aspect ratio
- Use the up/down arrows to make the image Width between 10.4 and 10.5 inches
- Click OK
- Click File: Print
- Return to SpinWorks for more processing
It might be a good idea to save your Word file so that you can print and/or adjust it later as needed.
Tutorial note: This ends the step-by-step guide through the tutorial. At this point, you can choose between the following: save your data and quit SpinWorks (don't forget to log out of the computer so that you are not billed for more printing), or add more data to your spectrum (peak picks, integrals, inset boxes) and print expanded spectra. To get instructions for the latter, select a section from the Table of Contents.
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created 10/2005 by Alan Shusterman
